This experiment determined the concentration of phosphorus in two different water samples, alpha (α) and theta (∆), using both Persulfate Digestion Method for Total Phosphorus and Acid Hydrolysis for Condensed Phosphates. The analysis revealed a significantly higher phosphorus concentration in sample alpha compared to theta. Both samples exhibited an absorption wavelength of 690nm. A strong correlation between light absorption with regard to cobalt (II) chloride and the phosphorus concentration was observed, highlighting the effectiveness of spectrophotometry for accurate measurements.