Assignment on SciFinder Experiment

The course work involves producing a retrosynthetic analysis for a given problem structure, exploring synthetic strategies, justifying the preferred strategy, and identifying references using SciFinder.

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Added on 2021-04-17

Assignment on SciFinder Experiment

Added on 2021-04-17

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SCINFINDER EXPERIMENTContentsAbstract......................................................................................................................................................21.0 Introduction.........................................................................................................................................22.0 Methods................................................................................................................................................23.0 Procedure.............................................................................................................................................24.0 Results..................................................................................................................................................25.0 Discussion.............................................................................................................................................36.0 Conclusion............................................................................................................................................5References..................................................................................................................................................5

AbstractScinfinder experiment involve molecules which are found in carbonyl compounds. The compound contain OH group or CoH group. This compounds are involved in reaction mechanism.

1.0 IntroductionScinfinder contain reaction mechanism which involve number of molecules in carbonyl groups . The carbonyl include NH , OH and charity center. Charity are group of compounds that are involved in reaction mechanism during charity. Chyrol center is the one which accepts racemic synthesis.2.0 MethodsReagents.A solution of one mole carbonyl compound2ml of tetrahydrofuran2ml of Calcium 0.5 ml complex one benzene15ml of esterSodium hydroxide Aluminum compoundAnhydrous Sodium sulphateChromatography3.0 Procedure.2ml of Ca 0.5 complex in benzene was added to a solution of one mole carbonyl compound in 2.5 ml of tetrahydrofuran. For about 5 minutes 15ml of ester was added followed by seven drops of aqueous base and stir was to done to destroy activated aluminum compound. The resultant mixture is dried with anhydrous Sodium sulphate. This was followed by filtration in order to separate the solid and Cen traded . Chromatography was to be done by alumina by using 3 percent ester in pentene for purification to occur .The process continued by addition of try-methylamine through chromatography in order to get the product results.4.0 ResultsAt the beginning of the experiment when complex obenzene was added to a solution of one moleof carbonyl compound there was no reaction. This was due to absent of the catalyst that may splitmolecule of carbonyl compound for the reaction to occur. Heating of a solution for about 30 minutes increases the cativation energy in the solution hence occurrence of the reaction.

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